Kinetic Study by Proton Nuclear Magnetic Resonance Spectroscopy of the Reaction between Ethyl Pyruvate and Diethyl Phosphite Yielding 2-Diethoxyphosphonyl-2-Hydroxypropionic Acid Ethyl Ester.

microstructural investigation and molecularweight determination of 1, 2-polybutadiene by nuclear magnetic resonance spectroscopy

in this research, the microstructural of low molecular weight 1,2-polybutadiene (1,2-pbd) was conducted by 1h and 13c nuclear magnetic resonance spectroscopy (nmr) to determine the isomeric contents of 1,4-cis, 1,4-trans and 1,2-vinyl in 1,2-pbd polymer structures. number average molecular weight for low molecular weight 1,2-pbd was measured by nmr techniques and the results were compared with ...

Proton Nuclear Magnetic Resonance Spectroscopy

threo-Diethyl 2-ethyl-2-hy­droxy-3-(4-methyl­benzene­sulfonamido)­succinate

The asymmetric unit of the title compound, C(17)H(25)NO(7)S, contains two independent mol-ecules, which are enanti-omers forming a hydrogen-bonded dimer associated with two R(2) (2)(7) patterns. In each mol-ecule, one ethyl group from the two available ethyl ester functional groups is disordered. In one mol-ecule, the ethyl group of the ester function from an α-carb-oxy-lic acid is positionally...

Synthesis of MgO Nanoparticales and Identificationof Their Destructive Reaction Products by 2-Chloroethyl Ethyl Sulfide

Nanocrystalline magnesium oxides were prepared by sol–gel method and were characterized by X-ray diffraction, N2-BET, SEM and infrared spectroscopy techniques. The results confirmed the formation of Nano- MgO materials with crystallite size in range of 5-20 nm and surface areas of 336-556m2/g. The product has been tested as destructive adsorbent for the decontamination of (2-chloroethyl) et...

Quantification of plasma lipoproteins by proton nuclear magnetic resonance spectroscopy.

A new analytical procedure for quantifying plasma lipoproteins by proton nuclear magnetic resonance (NMR) spectroscopy has been developed that potentially offers significant advantages over existing clinical methods used for assessing risk of coronary heart disease. Analysis of a single spectrum of a nonfasting plasma sample, acquired simply and rapidly at moderate magnetic field strength (250 ...